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http://repository.aaup.edu/jspui/handle/123456789/759
Title: | Differential Pulse Polarography applied to Aromatic Disculfides |
Authors: | j. a. cox ali z. abu zuhri |
Issue Date: | 1988 |
Publisher: | Analyst |
Abstract: | The differential-pulse polarographic behaviour of p-tolyl disulphide, 3-nitrophenyl disulphide and benzyl disulphide was investigated as a function of pH and concentration. At pH 11.4, with a 50% methanol solution as the solvent, a linear relationship between peak current and concentration was obtained for each compound over at least two orders of magnitude at a static mercury drop electrode; the detection limits were 0.2 µM in each instance. The pre-wave observed in the reduction of p-tolyl disulphide and 3-nitrophenyl disulphide was shown to be caused by chemical reactions with mercury rather than by simple adsorption. |
URI: | http://repository.aaup.edu/jspui/handle/123456789/759 |
Appears in Collections: | Faculty & Staff Scientific Research publications |
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